Jump to content
Main menu
Main menu
move to sidebar
hide
Navigation
Main page
Recent changes
Random page
Help about MediaWiki
Special pages
Niidae Wiki
Search
Search
Appearance
Create account
Log in
Personal tools
Create account
Log in
Pages for logged out editors
learn more
Contributions
Talk
Editing
Titration
(section)
Page
Discussion
English
Read
Edit
View history
Tools
Tools
move to sidebar
hide
Actions
Read
Edit
View history
General
What links here
Related changes
Page information
Appearance
move to sidebar
hide
Warning:
You are not logged in. Your IP address will be publicly visible if you make any edits. If you
log in
or
create an account
, your edits will be attributed to your username, along with other benefits.
Anti-spam check. Do
not
fill this in!
===Preparation techniques=== Typical titrations require titrant and analyte to be in a liquid (solution) form. Though solids are usually dissolved into an aqueous solution, other solvents such as [[Acetic acid|glacial acetic acid]] or [[ethanol]] are used for special purposes (as in [[petrochemistry]], which specializes in petroleum.)<ref> {{Cite book | last = Matar | first = S. |author2=L.F. Hatch | title = Chemistry of Petrochemical Processes | publisher = Gulf Professional Publishing | edition = 2 | year = 2001 | isbn = 0-88415-315-0 }}</ref> Concentrated analytes are often diluted to improve accuracy. Many non-acidβbase titrations require a constant [[pH]] during the reaction. Therefore, a [[buffer solution]] may be added to the titration chamber to maintain the pH.<ref> {{Cite book | last = Verma | first = Dr. N.K. |author2=S.K. Khanna |author3=Dr B. Kapila | title = Comprehensive Chemistry XI | publisher = Laxmi Publications | location = New Delhi | pages = 642β645 | isbn = 81-7008-596-9 }}</ref> In instances where two reactants in a sample may react with the titrant and only one is the desired analyte, a separate [[Masking agent|masking solution]] may be added to the reaction chamber which eliminates the effect of the unwanted ion.<ref> {{Cite book | last = Patnaik | first = P. | title = Dean's Analytical Chemistry Handbook | publisher = McGraw-Hill Prof Med/Tech | edition = 2 | year = 2004 | pages = 2.11β2.16 | isbn = 0-07-141060-0 }}</ref> Some reduction-oxidation ([[redox]]) reactions may require heating the sample solution and titrating while the solution is still hot to increase the [[reaction rate]]. For instance, the oxidation of some oxalate solutions requires heating to {{convert|60|C|F}} to maintain a reasonable rate of reaction.<ref> {{Cite book | last = Walther | first = J.V. | title = Essentials of Geochemistry | publisher = Jones & Bartlett Learning | year = 2005 | pages = 515β520 | isbn = 0-7637-2642-7 }}</ref>
Summary:
Please note that all contributions to Niidae Wiki may be edited, altered, or removed by other contributors. If you do not want your writing to be edited mercilessly, then do not submit it here.
You are also promising us that you wrote this yourself, or copied it from a public domain or similar free resource (see
Encyclopedia:Copyrights
for details).
Do not submit copyrighted work without permission!
Cancel
Editing help
(opens in new window)
Search
Search
Editing
Titration
(section)
Add topic